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High-Resolution Electron Microscopy$
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John C. H. Spence

Print publication date: 2008

Print ISBN-13: 9780199552757

Published to Oxford Scholarship Online: January 2010

DOI: 10.1093/acprof:oso/9780199552757.001.0001

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EXPERIMENTAL METHODS

EXPERIMENTAL METHODS

Chapter:
(p.318) 12 EXPERIMENTAL METHODS
Source:
High-Resolution Electron Microscopy
Author(s):

JOHN C. H. SPENCE

Publisher:
Oxford University Press
DOI:10.1093/acprof:oso/9780199552757.003.0012

This chapter focuses on the practical problems encountered when attempting to record atomic-resolution images. The human skills of sample alignment, focusing, astigmatism correction, and image recording (at the right moment) are described using a worked example. Autotuning software is discussed, in addition to the choice of substrate film. The chapter ends with a summary of ancillary equipment and a check-list.

Keywords:   experimental technique, astigmatism correction, focussing methods, autotuning, alignment methods

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